Mn1—O1 | 1.817 (3) | C15—C16 | 1.3900 |
Mn1—O1i | 1.821 (3) | C15—H15 | 0.9500 |
Mn1—N1 | 2.187 (5) | C16—H16 | 0.9500 |
Mn1—N2 | 2.092 (3) | C11B—C12B | 1.3900 |
Mn1—N3 | 2.178 (3) | C11B—C16B | 1.3900 |
Mn1—N4 | 2.116 (3) | C12B—C13B | 1.3900 |
Mn1—Mn1i | 2.7211 (13) | C12B—H12B | 0.9500 |
N1—C1 | 1.478 (6) | C13B—C14B | 1.3900 |
N1—C10 | 1.485 (7) | C13B—H13B | 0.9500 |
N1—H1 | 0.9300 | C14B—C15B | 1.3900 |
N2—C3 | 1.482 (5) | C14B—H14B | 0.9500 |
N2—C2 | 1.484 (6) | C15B—C16B | 1.3900 |
N2—H2 | 0.9300 | C15B—H15B | 0.9500 |
N3—C6 | 1.456 (5) | C16B—H16B | 0.9500 |
N3—C5 | 1.488 (5) | C17—C18 | 1.399 (5) |
N3—H3 | 0.9300 | C17—C22 | 1.399 (5) |
N4—C8 | 1.450 (6) | C18—C19 | 1.385 (5) |
N4—C7 | 1.495 (6) | C18—H18 | 0.9500 |
N4—H4 | 0.9300 | C19—C20 | 1.380 (6) |
C1—C2 | 1.497 (6) | C19—H19 | 0.9500 |
C1—H1B | 0.9900 | C20—C21 | 1.379 (5) |
C1—H1C | 0.9900 | C20—H20 | 0.9500 |
C2—H2A | 0.9900 | C21—C22 | 1.382 (5) |
C2—H2B | 0.9900 | C21—H21 | 0.9500 |
C3—C4 | 1.492 (6) | C22—H22 | 0.9500 |
C3—H3A | 0.9900 | C23—C24 | 1.393 (5) |
C3—H3B | 0.9900 | C23—C28 | 1.404 (5) |
C4—C5 | 1.511 (6) | C24—C25 | 1.398 (5) |
C4—H4A | 0.9900 | C24—H24 | 0.9500 |
C4—H4B | 0.9900 | C25—C26 | 1.379 (6) |
C5—H5A | 0.9900 | C25—H25 | 0.9500 |
C5—H5B | 0.9900 | C26—C27 | 1.379 (5) |
C6—C7 | 1.484 (7) | C26—H26 | 0.9500 |
C6—H6A | 0.9900 | C27—C28 | 1.387 (5) |
C6—H6B | 0.9900 | C27—H27 | 0.9500 |
C7—H7A | 0.9900 | C28—H28 | 0.9500 |
C7—H7B | 0.9900 | C29—C30 | 1.391 (5) |
C8—C9 | 1.503 (7) | C29—C34 | 1.395 (5) |
C8—H8A | 0.9900 | C30—C31 | 1.396 (5) |
C8—H8B | 0.9900 | C30—H30 | 0.9500 |
C9—C10 | 1.516 (7) | C31—C32 | 1.375 (5) |
C9—H9A | 0.9900 | C31—H31 | 0.9500 |
C9—H9B | 0.9900 | C32—C33 | 1.372 (6) |
C10—H10A | 0.9900 | C32—H32 | 0.9500 |
C10—H10B | 0.9900 | C33—C34 | 1.389 (5) |
B1—C23 | 1.639 (5) | C33—H33 | 0.9500 |
B1—C17 | 1.649 (5) | C34—H34 | 0.9500 |
B1—C29 | 1.651 (5) | N5—C35 | 1.146 (11) |
B1—C11B | 1.672 (6) | C35—C36 | 1.411 (11) |
B1—C11 | 1.705 (6) | C36—H36A | 0.9800 |
C11—C12 | 1.3900 | C36—H36B | 0.9800 |
C11—C16 | 1.3900 | C36—H36C | 0.9800 |
C12—C13 | 1.3900 | N5B—C35B | 1.129 (11) |
C12—H12 | 0.9500 | C35B—C36B | 1.454 (12) |
C13—C14 | 1.3900 | C36B—H36D | 0.9800 |
C13—H13 | 0.9500 | C36B—H36E | 0.9800 |
C14—C15 | 1.3900 | C36B—H36F | 0.9800 |
C14—H14 | 0.9500 | ||
O1—Mn1—O1i | 83.18 (11) | C17—B1—C11B | 106.0 (4) |
O1—Mn1—N1 | 100.05 (14) | C29—B1—C11B | 105.6 (3) |
O1—Mn1—N2 | 174.88 (13) | C23—B1—C11 | 105.4 (3) |
O1—Mn1—N3 | 95.63 (12) | C17—B1—C11 | 111.8 (3) |
O1—Mn1—N4 | 90.76 (13) | C29—B1—C11 | 110.7 (3) |
O1i—Mn1—N1 | 97.81 (13) | C12—C11—C16 | 120.0 |
O1i—Mn1—N2 | 91.73 (13) | C12—C11—B1 | 121.2 (3) |
O1i—Mn1—N3 | 97.79 (12) | C16—C11—B1 | 118.8 (3) |
O1i—Mn1—N4 | 173.47 (12) | C13—C12—C11 | 120.0 |
N1—Mn1—N2 | 80.14 (14) | C13—C12—H12 | 120.0 |
N1—Mn1—N3 | 159.04 (14) | C11—C12—H12 | 120.0 |
N1—Mn1—N4 | 85.59 (15) | C12—C13—C14 | 120.0 |
N2—Mn1—N3 | 85.49 (13) | C12—C13—H13 | 120.0 |
N2—Mn1—N4 | 94.35 (14) | C14—C13—H13 | 120.0 |
N3—Mn1—N4 | 80.34 (14) | C15—C14—C13 | 120.0 |
Mn1—O1—Mn1i | 96.82 (11) | C15—C14—H14 | 120.0 |
C1—N1—C10 | 112.3 (4) | C13—C14—H14 | 120.0 |
C1—N1—Mn1 | 108.9 (3) | C14—C15—C16 | 120.0 |
C10—N1—Mn1 | 119.8 (4) | C14—C15—H15 | 120.0 |
C1—N1—H1 | 104.8 | C16—C15—H15 | 120.0 |
C10—N1—H1 | 104.8 | C15—C16—C11 | 120.0 |
Mn1—N1—H1 | 104.8 | C15—C16—H16 | 120.0 |
C3—N2—C2 | 110.2 (3) | C11—C16—H16 | 120.0 |
C3—N2—Mn1 | 116.2 (2) | C12B—C11B—C16B | 120.0 |
C2—N2—Mn1 | 107.2 (3) | C12B—C11B—B1 | 115.4 (4) |
C3—N2—H2 | 107.7 | C16B—C11B—B1 | 124.5 (4) |
C2—N2—H2 | 107.7 | C13B—C12B—C11B | 120.0 |
Mn1—N2—H2 | 107.7 | C13B—C12B—H12B | 120.0 |
C6—N3—C5 | 112.2 (3) | C11B—C12B—H12B | 120.0 |
C6—N3—Mn1 | 109.4 (3) | C12B—C13B—C14B | 120.0 |
C5—N3—Mn1 | 119.7 (2) | C12B—C13B—H13B | 120.0 |
C6—N3—H3 | 104.7 | C14B—C13B—H13B | 120.0 |
C5—N3—H3 | 104.7 | C15B—C14B—C13B | 120.0 |
Mn1—N3—H3 | 104.7 | C15B—C14B—H14B | 120.0 |
C8—N4—C7 | 110.7 (4) | C13B—C14B—H14B | 120.0 |
C8—N4—Mn1 | 115.8 (3) | C14B—C15B—C16B | 120.0 |
C7—N4—Mn1 | 106.5 (2) | C14B—C15B—H15B | 120.0 |
C8—N4—H4 | 107.8 | C16B—C15B—H15B | 120.0 |
C7—N4—H4 | 107.8 | C15B—C16B—C11B | 120.0 |
Mn1—N4—H4 | 107.8 | C15B—C16B—H16B | 120.0 |
N1—C1—C2 | 106.8 (4) | C11B—C16B—H16B | 120.0 |
N1—C1—H1B | 110.4 | C18—C17—C22 | 113.6 (3) |
C2—C1—H1B | 110.4 | C18—C17—B1 | 124.2 (3) |
N1—C1—H1C | 110.4 | C22—C17—B1 | 122.2 (3) |
C2—C1—H1C | 110.4 | C19—C18—C17 | 123.4 (4) |
H1B—C1—H1C | 108.6 | C19—C18—H18 | 118.3 |
N2—C2—C1 | 107.9 (4) | C17—C18—H18 | 118.3 |
N2—C2—H2A | 110.1 | C20—C19—C18 | 120.8 (4) |
C1—C2—H2A | 110.1 | C20—C19—H19 | 119.6 |
N2—C2—H2B | 110.1 | C18—C19—H19 | 119.6 |
C1—C2—H2B | 110.1 | C21—C20—C19 | 117.7 (4) |
H2A—C2—H2B | 108.4 | C21—C20—H20 | 121.1 |
N2—C3—C4 | 113.0 (3) | C19—C20—H20 | 121.1 |
N2—C3—H3A | 109.0 | C20—C21—C22 | 120.7 (4) |
C4—C3—H3A | 109.0 | C20—C21—H21 | 119.7 |
N2—C3—H3B | 109.0 | C22—C21—H21 | 119.7 |
C4—C3—H3B | 109.0 | C21—C22—C17 | 123.8 (3) |
H3A—C3—H3B | 107.8 | C21—C22—H22 | 118.1 |
C3—C4—C5 | 113.3 (4) | C17—C22—H22 | 118.1 |
C3—C4—H4A | 108.9 | C24—C23—C28 | 114.8 (3) |
C5—C4—H4A | 108.9 | C24—C23—B1 | 125.1 (3) |
C3—C4—H4B | 108.9 | C28—C23—B1 | 120.2 (3) |
C5—C4—H4B | 108.9 | C23—C24—C25 | 122.8 (4) |
H4A—C4—H4B | 107.7 | C23—C24—H24 | 118.6 |
N3—C5—C4 | 112.7 (4) | C25—C24—H24 | 118.6 |
N3—C5—H5A | 109.1 | C26—C25—C24 | 120.1 (4) |
C4—C5—H5A | 109.1 | C26—C25—H25 | 119.9 |
N3—C5—H5B | 109.1 | C24—C25—H25 | 119.9 |
C4—C5—H5B | 109.1 | C25—C26—C27 | 119.2 (4) |
H5A—C5—H5B | 107.8 | C25—C26—H26 | 120.4 |
N3—C6—C7 | 108.2 (4) | C27—C26—H26 | 120.4 |
N3—C6—H6A | 110.1 | C26—C27—C28 | 119.8 (4) |
C7—C6—H6A | 110.1 | C26—C27—H27 | 120.1 |
N3—C6—H6B | 110.1 | C28—C27—H27 | 120.1 |
C7—C6—H6B | 110.1 | C27—C28—C23 | 123.4 (4) |
H6A—C6—H6B | 108.4 | C27—C28—H28 | 118.3 |
C6—C7—N4 | 109.0 (3) | C23—C28—H28 | 118.3 |
C6—C7—H7A | 109.9 | C30—C29—C34 | 114.1 (3) |
N4—C7—H7A | 109.9 | C30—C29—B1 | 125.2 (3) |
C6—C7—H7B | 109.9 | C34—C29—B1 | 120.7 (3) |
N4—C7—H7B | 109.9 | C29—C30—C31 | 123.2 (3) |
H7A—C7—H7B | 108.3 | C29—C30—H30 | 118.4 |
N4—C8—C9 | 112.1 (4) | C31—C30—H30 | 118.4 |
N4—C8—H8A | 109.2 | C32—C31—C30 | 120.2 (4) |
C9—C8—H8A | 109.2 | C32—C31—H31 | 119.9 |
N4—C8—H8B | 109.2 | C30—C31—H31 | 119.9 |
C9—C8—H8B | 109.2 | C33—C32—C31 | 118.7 (4) |
H8A—C8—H8B | 107.9 | C33—C32—H32 | 120.7 |
C8—C9—C10 | 116.1 (5) | C31—C32—H32 | 120.7 |
C8—C9—H9A | 108.3 | C32—C33—C34 | 120.0 (4) |
C10—C9—H9A | 108.3 | C32—C33—H33 | 120.0 |
C8—C9—H9B | 108.3 | C34—C33—H33 | 120.0 |
C10—C9—H9B | 108.3 | C33—C34—C29 | 123.7 (4) |
H9A—C9—H9B | 107.4 | C33—C34—H34 | 118.1 |
N1—C10—C9 | 113.5 (5) | C29—C34—H34 | 118.1 |
N1—C10—H10A | 108.9 | N5—C35—C36 | 178.4 (10) |
C9—C10—H10A | 108.9 | N5B—C35B—C36B | 178.2 (11) |
N1—C10—H10B | 108.9 | C35B—C36B—H36D | 109.5 |
C9—C10—H10B | 108.9 | C35B—C36B—H36E | 109.5 |
H10A—C10—H10B | 107.7 | H36D—C36B—H36E | 109.5 |
C23—B1—C17 | 108.1 (3) | C35B—C36B—H36F | 109.5 |
C23—B1—C29 | 109.1 (3) | H36D—C36B—H36F | 109.5 |
C17—B1—C29 | 111.6 (3) | H36E—C36B—H36F | 109.5 |
C23—B1—C11B | 116.5 (4) |