| Bruker SMART APEXII diffractometer | 6092 independent reflections |
| Radiation source: fine-focus sealed tube | 4083 reflections with I > 2σ(I) |
| graphite | Rint = 0.064 |
| Detector resolution: 8.3 pixels mm-1 | θmax = 25.3°, θmin = 2.8° |
| ω scans | h = −13→13 |
| Absorption correction: multi-scan (SADABS; Sheldrick, 1996) | k = −14→14 |
| Tmin = 0.952, Tmax = 0.972 | l = −16→16 |
| 17931 measured reflections |
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