| Bruker APEXII CCD diffractometer | 1935 independent reflections |
| Radiation source: fine-focus sealed tube | 1474 reflections with I > 2σ(I) |
| graphite | Rint = 0.036 |
| φ and ω scans | θmax = 25.5°, θmin = 2.7° |
| Absorption correction: multi-scan (SADABS; Bruker, 2004) | h = −10→11 |
| Tmin = 0.976, Tmax = 0.979 | k = −11→14 |
| 5880 measured reflections | l = −11→11 |