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. 2011 Jun 18;67(Pt 7):o1653–o1654. doi: 10.1107/S1600536811022306
Refinement on F2 Primary atom site location: structure-invariant direct methods
Least-squares matrix: full Secondary atom site location: difference Fourier map
R[F2 > 2σ(F2)] = 0.035 Hydrogen site location: inferred from neighbouring sites
wR(F2) = 0.082 H-atom parameters constrained
S = 0.99 w = 1/[σ2(Fo2) + (0.0509P)2] where P = (Fo2 + 2Fc2)/3
1695 reflections (Δ/σ)max < 0.001
228 parameters Δρmax = 0.19 e Å3
1 restraint Δρmin = −0.14 e Å3