| Bruker SMART APEXII CCD diffractometer | 11497 independent reflections |
| Radiation source: fine-focus sealed tube | 8871 reflections with I > 2σ(I) |
| graphite | Rint = 0.040 |
| φ and ω scans | θmax = 29.0°, θmin = 0.9° |
| Absorption correction: multi-scan (SADABS; Bruker, 2009) | h = −12→12 |
| Tmin = 0.965, Tmax = 0.983 | k = −13→13 |
| 44431 measured reflections | l = −31→31 |