| Rigaku Saturn70 diffractometer | 873 reflections with F2 > 2σ(F2) |
| Detector resolution: 14.629 pixels mm-1 | Rint = 0.057 |
| ω scans | θmax = 25.0° |
| Absorption correction: multi-scan (REQAB; Rigaku, 1998) | h = −9→11 |
| Tmin = 0.384, Tmax = 0.815 | k = −12→16 |
| 1716 measured reflections | l = −4→4 |
| 895 independent reflections |
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