| Bruker SMART APEX diffractometer | 3774 independent reflections |
| Radiation source: fine-focus sealed tube | 2730 reflections with I > 2σ(I) |
| graphite | Rint = 0.015 |
| φ and ω scans | θmax = 27.7°, θmin = 3.1° |
| Absorption correction: multi-scan (SADABS; Sheldrick, 1996) | h = −8→12 |
| Tmin = 0.947, Tmax = 0.984 | k = −21→16 |
| 7411 measured reflections | l = −12→13 |