Rigaku Saturn CCD area-detector diffractometer	6772 independent reflections
Radiation source: rotating anode	3380 reflections with I > 2σ(I)
multilayer	Rint = 0.047
Detector resolution: 7.31 pixels mm-1	θmax = 27.9°, θmin = 1.9°
ω and φ scans	h = −15→12
Absorption correction: multi-scan (CrystalClear; Rigaku/MSC, 2005)	k = −15→16
Tmin = 0.970, Tmax = 0.982	l = −16→13
12066 measured reflections