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. Author manuscript; available in PMC: 2011 Nov 22.
Published in final edited form as: Chemistry. 2010 Nov 22;16(44):13058–13062. doi: 10.1002/chem.201002157

Scheme 4.

Scheme 4

Attempted oxidative dimerization of 16 a. a) LHMDS, HMPA, THF, −78°C, 2 h; then [Cp2FePF6], −60°C, 72 h, 0 %. LHMDS = lithium bis(trimethylsilyl)amide, [Cp2FePF6] = ferrocenium hexafluorophosphate.