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Comparison of 13C chemical shifts of UQ-8 in DsbB/CuDMPE-DTPA and DsbB. Chemical shifts of UQ-8 in DsbB are from the previous study.21
| Chemical Shift (ppm) | UQ-8 in DsbB CuDMPE-DTPA | UQ-8 in DsbB21 |
|---|---|---|
| CH3 (5′) | 15.6 | 15.9 |
| CH3 (9′~37′) | 20.5~17.8 | 20.7~17.9 |
| CH3 (38) | 28.0 | 28.2 |
| CH2 (11~35) | 30.4~27.5 | 30.3~27.3 |
| CH2 (10~34) | 43.8~41.5 | 43.4~41.6 |
| CH3O (2′, 3′) | 63.2, 63.7 | 63.6, 64.0 |
| C=C (12~36) | 126.0~123.0 | 126.6~123.6 |
| C=C (13~37) | 138.6~135.0 | 139.0~135.2 |
| C=C (9) | 140.2 | 140.2 |
| C=O (1, 4) | 154.5 | 154.7 |
