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. Author manuscript; available in PMC: 2011 Dec 7.
Published in final edited form as: Phys Chem Chem Phys. 2010 Oct 8;12(45):14873–14883. doi: 10.1039/c0cp00795a

Figure 2.

Figure 2

Pulse sequence for the three-dimensional CSA/DIP orientational correlation experiment. Solid and blank squares denote π/2 and π pulses, respectively. 1H-15N dipolar coupling and 15N CSA interactions are reintroduced by the γ-encoded symmetry sequences R1817 and R1425/3 in the indirect t1 and t2 dimensions, respectively.