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. Author manuscript; available in PMC: 2012 Sep 2.
Published in final edited form as: J Org Chem. 2011 Aug 3;76(17):7195–7203. doi: 10.1021/jo201313a

Table 4.

Chlorodeboronation of Electron-Poor Potassium Aryltrifluoroborate with TCICA

graphic file with name nihms316337t22.jpg
entry product reaction
time		 % isolated
yield
1 graphic file with name nihms316337t23.jpg 2a 2 h 87
2 graphic file with name nihms316337t24.jpg 2b 1 h 92
3 graphic file with name nihms316337t25.jpg 2c 30 min 82
4 graphic file with name nihms316337t26.jpg 2d 40 min 80
5a graphic file with name nihms316337t27.jpg 2e 4 h 85
6a graphic file with name nihms316337t28.jpg 2f 6 h 89
a

reaction run at 80 °C.