Table 6.
entry | product | method | reaction time |
% isolated yield |
||
---|---|---|---|---|---|---|
1 | 3a | A | 40 min | 95 | ||
2 | 3b | A | 6 h | 80 | ||
3 | 3c | A | 2 h | 91 | ||
4 | 3d | A | 2 h | 90 | ||
5 | 3e | A | 2 h | 89 | ||
6 | 3f | A | 2 h | 95 | ||
7 | 3g | B | 1 h | 88 | ||
8 | 3h | B | 1 h | 91 | ||
9 | 3i | B | 30 min | 86 |
entry | product | method | reaction time |
% isolated yield |
||
---|---|---|---|---|---|---|
1 | 3a | A | 40 min | 95 | ||
2 | 3b | A | 6 h | 80 | ||
3 | 3c | A | 2 h | 91 | ||
4 | 3d | A | 2 h | 90 | ||
5 | 3e | A | 2 h | 89 | ||
6 | 3f | A | 2 h | 95 | ||
7 | 3g | B | 1 h | 88 | ||
8 | 3h | B | 1 h | 91 | ||
9 | 3i | B | 30 min | 86 |