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. Author manuscript; available in PMC: 2012 Sep 2.
Published in final edited form as: J Org Chem. 2011 Aug 3;76(17):7195–7203. doi: 10.1021/jo201313a

Table 6.

Chlorodeboronation of Potassium Heteroaryltrifluoroborate With TCICA

graphic file with name nihms316337t40.jpg

entry graphic file with name nihms316337t41.jpg product method reaction
time
% isolated
yield
1 graphic file with name nihms316337t42.jpg graphic file with name nihms316337t43.jpg 3a A 40 min 95
2 graphic file with name nihms316337t44.jpg graphic file with name nihms316337t45.jpg 3b A 6 h 80
3 graphic file with name nihms316337t46.jpg graphic file with name nihms316337t47.jpg 3c A 2 h 91
4 graphic file with name nihms316337t48.jpg graphic file with name nihms316337t49.jpg 3d A 2 h 90
5 graphic file with name nihms316337t50.jpg graphic file with name nihms316337t51.jpg 3e A 2 h 89
6 graphic file with name nihms316337t52.jpg graphic file with name nihms316337t53.jpg 3f A 2 h 95
7 graphic file with name nihms316337t54.jpg graphic file with name nihms316337t55.jpg 3g B 1 h 88
8 graphic file with name nihms316337t56.jpg graphic file with name nihms316337t57.jpg 3h B 1 h 91
9 graphic file with name nihms316337t58.jpg graphic file with name nihms316337t59.jpg 3i B 30 min 86