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. 2011 Jun 28;12(3):854–861. doi: 10.1208/s12249-011-9645-7

Table III.

Operating Conditions for Cycle Used to Measure Product Resistance

Lowest shelf temperature during freezing, °C −40
Shelf temperature during primary drying, °C −5
Chamber pressure during primary drying, Pa 10
Product temperature from thermocouple measurement, °C −22