Table 1.
Experimental results for the photodecarboxylation of 3.
| batch | μ-reactor | |
| time [h] | 1 | 1 |
| 4/5 ratioa | 87/13 | 81/19 |
| yield 4 [%]b | 29 | 47 |
aDetermined by 1H NMR analysis of the crude product. bIsolated yield after column chromatography.
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