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Experimental results for the photodecarboxylative addition of 11 to 2.
| batch | μ-reactor | |
| time [h] | 1 | 1 |
| conversion [%]a | 100 | 90 |
| 12/13 ratioa | 90/10 | 100/0 |
| yield 12 [%]b | 41 | n.d.c |
aDetermined by 1H NMR analysis of the crude product. bIsolated yield after column chromatography. cYield not determined.
