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. 2011 Aug 2;7:1064–1069. doi: 10.3762/bjoc.7.122

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Copyright © 2011, Nagaki et al.

This is an Open Access article under the terms of the Creative Commons Attribution License (https://creativecommons.org/licenses/by/2.0), which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.

The license is subject to the Beilstein Journal of Organic Chemistry terms and conditions: (https://www.beilstein-journals.org/bjoc/terms)

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Integrated flow microreactor system for oxidative homocoupling reaction of aryllithium with FeCl₃. T-shaped micromixer: M1 (inner diameter: 250 μm), M2 (inner diameter: 500 μm), and M3 (inner diameter: 500 μm), microtube reactor: R1, R2 and R3 ( = 1000 μm, length = 50 cm), a solution of aryl halides: 0.10 M in THF (6.0 mL/min), a solution of lithium reagent: 0.42 M in hexane (n-BuLi) or Et₂O (PhLi) (1.5 mL/min), a solution of FeCl₃: 0.10 M in THF (6 mL/min), a solution of methanol: Neat (1.5 mL/min).

Inline graphic — Integrated flow microreactor system for oxidative homocoupling reaction of aryllithium with FeCl₃. T-shaped micromixer: M1 (inner diameter: 250 μm), M2 (inner diameter: 500 μm), and M3 (inner diameter: 500 μm), microtube reactor: R1, R2 and R3 ( = 1000 μm, length = 50 cm), a solution of aryl halides: 0.10 M in THF (6.0 mL/min), a solution of lithium reagent: 0.42 M in hexane (n-BuLi) or Et₂O (PhLi) (1.5 mL/min), a solution of FeCl₃: 0.10 M in THF (6 mL/min), a solution of methanol: Neat (1.5 mL/min).