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. 2011 Aug 2;7:1064–1069. doi: 10.3762/bjoc.7.122

Table 1.

Homocoupling of aryl halides using the integrated flow microreactor system.

Ar–X T (°C) tR1 (s) Ar–Ar Yield (%)

graphic file with name Beilstein_J_Org_Chem-07-1064-i002.jpg 24 3.100 graphic file with name Beilstein_J_Org_Chem-07-1064-i003.jpg 72
graphic file with name Beilstein_J_Org_Chem-07-1064-i004.jpg 24 3.100 graphic file with name Beilstein_J_Org_Chem-07-1064-i005.jpg 69
graphic file with name Beilstein_J_Org_Chem-07-1064-i006.jpg 0 3.100 graphic file with name Beilstein_J_Org_Chem-07-1064-i007.jpg 76
graphic file with name Beilstein_J_Org_Chem-07-1064-i008.jpg −28 0.055 graphic file with name Beilstein_J_Org_Chem-07-1064-i009.jpg 75
graphic file with name Beilstein_J_Org_Chem-07-1064-i010.jpg 0 0.055 graphic file with name Beilstein_J_Org_Chem-07-1064-i011.jpg 66
graphic file with name Beilstein_J_Org_Chem-07-1064-i012.jpg 24 0.055 graphic file with name Beilstein_J_Org_Chem-07-1064-i013.jpg 76
graphic file with name Beilstein_J_Org_Chem-07-1064-i014.jpg −48 0.014 graphic file with name Beilstein_J_Org_Chem-07-1064-i015.jpg 53a
graphic file with name Beilstein_J_Org_Chem-07-1064-i016.jpg −48 0.014 graphic file with name Beilstein_J_Org_Chem-07-1064-i017.jpg 63a

aPhLi instead of n-BuLi was used as lithiating reagent.