Table 1.
Homocoupling of aryl halides using the integrated flow microreactor system.
Ar–X | T (°C) | tR1 (s) | Ar–Ar | Yield (%) |
![]() |
24 | 3.100 | ![]() |
72 |
![]() |
24 | 3.100 | ![]() |
69 |
![]() |
0 | 3.100 | ![]() |
76 |
![]() |
−28 | 0.055 | ![]() |
75 |
![]() |
0 | 0.055 | ![]() |
66 |
![]() |
24 | 0.055 | ![]() |
76 |
![]() |
−48 | 0.014 | ![]() |
53a |
![]() |
−48 | 0.014 | ![]() |
63a |
aPhLi instead of n-BuLi was used as lithiating reagent.