Table 1.
Sample name | Ret time min | Area Mv min | Height Mv | Amount ppb | % of recovery |
---|---|---|---|---|---|
Std 2.0 ppb | 5.48 | 221,323 | 878,118 | 2.00001 | 100 |
Std 1.0 ppb | 5.49 | 110,008 | 43,988 | 1.0003 | 100 |
Std 0.5 ppb | 5.47 | 54,896 | 219,905 | 0.4985 | 99.7 |
Std 0.25 ppb | 5.48 | 27,419 | 111,156 | 0.2504 | 100.16 |
Spiked milk | |||||
2.5 ppb (1) | 5.57 | 55,298 | 246,355 | 2.23 | 89 |
(2) | 5.57 | 56,604 | 256,889 | 2.33 | 93 |
(3) | 5.57 | 59,533 | 27,180 | 2.58 | 103 |
HPLC=High-performance liquid chromatography;
min=Minutes;
Mv=Measurement unit;
Ret=Retention;
Std=Standard; 1, 2, and 3 with 2.5 ppb indicate replicate 1, 2, and 3