TABLE 1.
Data collection and refinement statistics
Values in parentheses are for the highest resolution shell. Ramachandran statistics indicate the fraction of residues in the most favored/allowed/disallowed regions, respectively.
| Data collection | |
| Space group | P212121 |
| Cell dimensions | |
| a (Å) | 61.8 |
| b (Å) | 76.0 |
| c (Å) | 37.0 |
| Resolution range (Å) | 50.0–2.00 (2.07–2.00) |
| Observed reflections | 83,976 |
| Unique reflections | 12,160 |
| Rmerge | 0.073 (0.175) |
| Completeness (%) | 97.5 (94.9) |
| <I>/σ<I> | 19.6 (14.7) |
| Refinement | |
| Resolution range (Å) | 20.0–2.00 |
| R/Rfree | 0.162/0.204 |
| Root mean square deviation bond distances (Å)/angles (°) | 0.009/1.091 |
| Ramachandran statistics (%) | 88.8/11.2/0 |
| Protein Data Bank ID code | 3AYU |