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. Author manuscript; available in PMC: 2011 Oct 12.
Published in final edited form as: Org Lett. 2009 Feb 19;11(4):943–946. doi: 10.1021/ol802930q

Table 6.

β,β-difluoroamine synthesis via organocatalysis

graphic file with name nihms91352t26.jpg
cmpda product yield (%)b
18a graphic file with name nihms91352t27.jpg 64
18b graphic file with name nihms91352t28.jpg 67
18c graphic file with name nihms91352t29.jpg 77
18d graphic file with name nihms91352t30.jpg 68
a

All reactions were performed on a 0.05 mmol scale and proceeded to complete conversion.

b

Yield after chromatography