Table 1.
Dy3+ | Tb3+ | Er3+ | Tm3+ | |
---|---|---|---|---|
Δχ bax | 22.7 ± 1.3 | 29.2 ± 1.7 | −7.7 ± 0.7 | −17.5 ± 1.6 |
Δχ brh | 17.6 ± 0.7 | 16.9 ± 0.5 | −7.3 ± 0.2 | −17.1 ± 0.5 |
αc | 106 | 97 | 104 | 99 |
βc | 57 | 52 | 57 | 65 |
γc | 53 | 34 | 36 | 27 |
aΔχ-tensor parameters were determined relative to the conformer 1 of the family of NMR structures of Grb2 SH2 (1x0n.pdb). Metal ion coordinates were x = − 12.9, y = − 5.3, z = − 4.9
bΔχ ax and Δχ rh values are in 10−32 (m3) and error estimates were obtained by the Monte-Carlo protocol using 100 partial PCS data sets in which 30% of the input data were randomly deleted
cEuler angle rotations in ZYZ convention (degrees)