| Bruker SMART APEX CCD diffractometer | 2157 independent reflections |
| Radiation source: fine-focus sealed tube | 1294 reflections with I > 2σ(I) |
| graphite | Rint = 0.065 |
| phi and ω scans | θmax = 25.0°, θmin = 2.0° |
| Absorption correction: multi-scan (SADABS; Sheldrick, 1996) | h = −12→12 |
| Tmin = 0.982, Tmax = 0.985 | k = −17→14 |
| 6155 measured reflections | l = −9→9 |
Official websites use .gov
A
.gov website belongs to an official
government organization in the United States.
Secure .gov websites use HTTPS
A lock (
) or https:// means you've safely
connected to the .gov website. Share sensitive
information only on official, secure websites.