| Bruker APEXII DUO CCD area-detector diffractometer | 3990 independent reflections |
| Radiation source: fine-focus sealed tube | 2813 reflections with I > 2σ(I) |
| graphite | Rint = 0.041 |
| φ and ω scans | θmax = 30.2°, θmin = 1.6° |
| Absorption correction: multi-scan (SADABS; Bruker, 2009) | h = −19→19 |
| Tmin = 0.913, Tmax = 0.985 | k = −14→14 |
| 21164 measured reflections | l = −14→14 |