Table 1.
Batch 1 | Batch 2 | Batch 3 | Average | %RSD | |
---|---|---|---|---|---|
%C (w/w) a | 31.6 | 29.5 | 30.7 | 30.6 | 3 |
Plate count/m b | 45,800 | 46,300 | 52,400 | 48,200 | 8 |
Symmetry c | 0.6 | 0.6 | 0.6 | 0.6 | 3 |
k of nitrohexane d | 5.9 | 4.9 | 4.9 | 5.2 | 11 |
k of toluene e | 1.3 | 1.4 | 1.5 | 1.4 | 7 |
k of nitrobenzene e | 4.9 | 3.9 | 4.7 | 4.5 | 12 |
16 h CVD at 700 °C with hexane as source.
Plate count from nitrohexane.
Symmetry based on nitrohexane, LC conditions: F = 0.4 ml/min., T = 40 °C,
35/65 MeCN/water,
50/50 MeCN/water; All packed in 33 × 2.1 mm id. column.