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. Author manuscript; available in PMC: 2012 Mar 11.
Published in final edited form as: J Chromatogr A. 2011 Jan 5;1218(10):1359–1366. doi: 10.1016/j.chroma.2010.12.114

Table 1.

Repeatability of the carbon deposition process

Batch 1 Batch 2 Batch 3 Average %RSD
%C (w/w) a 31.6 29.5 30.7 30.6 3
Plate count/m b 45,800 46,300 52,400 48,200 8
Symmetry c 0.6 0.6 0.6 0.6 3
k of nitrohexane d 5.9 4.9 4.9 5.2 11
k of toluene e 1.3 1.4 1.5 1.4 7
k of nitrobenzene e 4.9 3.9 4.7 4.5 12
a

16 h CVD at 700 °C with hexane as source.

b

Plate count from nitrohexane.

c

Symmetry based on nitrohexane, LC conditions: F = 0.4 ml/min., T = 40 °C,

d

35/65 MeCN/water,

e

50/50 MeCN/water; All packed in 33 × 2.1 mm id. column.