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. Author manuscript; available in PMC: 2011 Nov 3.
Published in final edited form as: J AOAC Int. 2007 Jan-Feb;90(1):68–81.

Table 10.

Synephrine repeatability results

Materiala nb Result, μg/g SDc, μg/g RSD, % PRSDd, % HorRat
A 20 8290 123 1.48 4.10 0.36
B 20 26110 439 1.68 3.46 0.49
C 20 66580 1585 2.36 3.00 0.79
D 20 292300 6898 2.37 2.41 0.99
E 20 11980 432 3.55 3.88 0.91
F 20 4686 80.3 1.71 4.47 0.38
a

A = NIST bitter orange fruit powder, B = Nutratech C. aurantium dried fruit, C = NIST bitter orange extract 6% synephrine, D = Nutratech C. aurantium extract 30% synephrine, E = Product A capsules, F = Product B tablets.

b

n = Total number of samples tested.

c

SD = Standard deviation.

d

PRSD = Predicted relative standard deviation.