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. Author manuscript; available in PMC: 2011 Nov 3.
Published in final edited form as: J AOAC Int. 2007 Jan-Feb;90(1):68–81.

Table 12.

N-methyltyramine repeatability results

Materiala nb Result, μg/g SDc, μg/g RSD, % PRSDd, % HorRat
A 20 <300 NA NA NA NA
B 20 1321 48.8 3.70 5.41 0.68
C 20 5464 575 10.2 4.37 2.3
D 20 9326 1960 19.5 4.03 4.8
E 20 1667 156 8.95 5.22 1.7
F 20 <300 NA NA NA NA
a

A = NIST bitter orange fruit powder, B = Nutratech C. aurantium dried fruit, C = NIST bitter orange extract 6% synephrine, D = Nutratech C. aurantium extract 30% synephrine, E = Product A capsules, F = Product B tablets.

b

n = Total number of samples tested.

c

SD = Standard deviation.

d

PRSD = Predicted relative standard deviation.