Table 5.

NIST bitter orange fruit powder recovery

Compound	ASE, μg/g	Sonication, μg/g	Recovery, %	RSDa, %
Octopamine	158b	148b	93.6b	9.25
Synephrine	8610	8270	96.0	1.30
Phenylephrine	193b	NDc	0	NAd
Tyramine	75b	NDc	0	NAd
N-methyltyramine	146b	NDc	0	NAd
Hordenine	22b	NDc	0	NAd

^aRSD = Relative standard deviation; estimated from 5 replicate sample preparations.

^bResult below the limit of quantification for the method.

^cND = None detected.

^dNA = Not applicable.