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. Author manuscript; available in PMC: 2011 Nov 3.
Published in final edited form as: J AOAC Int. 2007 Jan-Feb;90(1):68–81.

Table 7.

Recovery of biogenic amines from dietary supplement negative control (low level)

Compound Amount added, μg Amount recovered, μg Recovery, % RSDa, %
Octopamine 101.6 101.1 99.5 1.24
Synephrine 111.5 115.8 104 1.36
Phenylephrine 107.1 128.8 120 3.44
Tyramine 99.73 117.1 117 0.52
N-methyltyramine 84.94 77.0 90.7 1.12
Hordenine 89.98 96.15 107 4.95
a

RSD = Relative standard deviation; estimated from triplicate determinations.