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. Author manuscript; available in PMC: 2011 Nov 3.
Published in final edited form as: J AOAC Int. 2007 Jan-Feb;90(1):68–81.

Table 9.

Recovery of biogenic amines from dietary supplement negative control (high level)

Compound Amount added, μg Amount recovered, μg Recovery, % RSDa, %
Octopamine 3946 3903 98.9 0.554
Synephrine 5080 4991 98.3 0.439
Phenylephrine 4802 4664 97.1 0.349
Tyramine 4628 4438 95.9 0.298
N-methyltyramine 751.2 737.7 98.2 0.441
Hordenine 3737 3703 99.1 0.387
a

RSD = Relative standard deviation; estimated from triplicate determinations.