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Results from 13C NMR and MALDI-TOF Mass Spectrometry.
| Sample | 13C NMR | MALDI-TOF | |||
|---|---|---|---|---|---|
| DB | DPn | Mn | Mn | Mw/Mn | |
| HPG-1 | 0.48 | 16.3 | 1341 | 1367 | 1.15 |
| HPG-2 | 0.50 | 18.1 | 1473 | 1257 | 1.18 |
| HPG-3+ | 0.57 | 10.9 | 672 | 890 | 1.23 |
HPG-3 was prepared from S-glycidol. All other HPG samples were prepared from the racemic version of glycidol.
