Skip to main content

View full-text article in PMC

. 2011 Sep 30;289(15):1757–1767. doi: 10.1007/s00396-011-2515-8

Table 1.

Chemical compositions of synthesised linear polyurethanes and results from WAXS analysis

Sample no.	Type of diisocyanate	Type of polyol	Type of chain extender	Two theta angles, grad	Crystallisation degree, %	Two theta angle, grad	Crystallisation degree, %
Sample no.	Type of diisocyanate	Type of polyol	Type of chain extender	Synthesis in dioxane		Synthesis in chlorobenzene
PU-1	MDI	POG 2,000	N-MDA	19.48, 23.61	23.31	19.52, 23.64	25.80
				26.81, 27.52		26.94, 29.83
				29.76, 36.17		36.22, 43.59
				21.02, 44.62		21.48, 44.65
PU-2			N-BDA
PU-3			TFBD	19.34,23.47	19.16
				26.72,36.03
				61.61,20.89
				44.28,
PU-4		POG 600	BD	6.7, 29.17	4.92
				29.49, 39.21
				42.95, 47.32
				48.32, 57.21
				65.1, 20.79
				44.32
PU-5			TFBD
PU-6	IPDI	POG 2,000	BD			19.41, 23.54	34.06
						26.79, 36.12
						43.07, 49.53
						20.43
PU-7			N-MDA
PU-8			N-BDA
PU-9	TDI	POG 2,000	BD			19.25, 23.37	31.82
						26.55, 29.14
						35.92, 39.15
						42.9, 47.25
						48.27, 50.23
						57.16, 60.77
						20.35
PU-10	HDI	POG 2,000	BD
PU-11	HDI	POG 2,000	N-MDA