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. 2011 Oct 19;5:427–433. doi: 10.2147/DDDT.S24504

Table 4.

Summary of stability data of ibuprofen under freeze–thaw conditions expressed as recovery (%)

Ibuprofen concentration (μg/mL)
4.0 μg/mL (%) recovery 8.0 μg/mL (%) recovery
Zero time (n = 3) 102.77 101.09
Cycle 1 (n = 3) 102.33 99.27
Cycle 2 (n = 3) 99.96 100.94
Cycle 3 (n = 3) 103.05 101.10