(b).
Crystals 4, 5 and 6. X-ray source: SER-CAT 22-ID; X-ray optics: monochromator; detector: Mar 225 CCD; wavelength: 2.0 Å; space group: I213.
| Crystal 4 | Crystal 5 | Crystal 6 | ||||
|---|---|---|---|---|---|---|
| Cell dimensions: a = b = c (Å) | 77.84 | 78.58 | 77.76 | |||
| Exposure (s) | 9.0 | 3.0 | 9.0 | 3.0 | 9.0 | 3.0 |
| Scan range (°) | 90.0 | 3 × 90.0 | 90.0 | 3 × 90.0 | 90.0 | 3 × 90.0 |
| Resolution (Å)‡ | 50.00–2.30 (2.38–2.30) | 50.00–2.30 (2.38–2.30) | 50.00–2.30 (2.38–2.30) | 50.00–2.30 (2.38–2.30) | 50.00–2.30 (2.38–2.30) | 50.00–2.30 (2.38–2.30) |
| Rsym (%) | 5.2 (8.9) | 6.5 (12.1) | 5.3 (7.7) | 5.8 (10.0) | 5.1 (11.1) | 6.7 (17.6) |
| I/σI | 62.3 (45.3) | 89.4 (58.0) | 69.8 (55.1) | 106.5 (69.8) | 58.2 (37.5) | 105.7 (96.0) |
| Completeness (%) | 99.24 (99.14) | 99.38 (99.19) | 99.14 (99.05) | 99.36 (99.19) | 99.46 (99.30) | 99.41 (99.29) |
| Redundancy | 10.3 | 30.8 | 10.2 | 30.3 | 10.3 | 30.4 |
†
Numbers in parentheses are statistics for the highest-resolution shell.
‡
Data were processed with ‘d*TREK’ then scaled by ‘3DSCALE’ software.