Table 2. Data-collection and structure-solution statistics.
Diffraction source | Rigaku RU-H3R rotating anode |
Diffraction protocol | Single wavelength |
Monochromator | Rotating copper anode |
Wavelength () | 1.5418 |
Detector | Rigaku R-AXIS IV++ image plate |
Temperature (K) | 93 |
Resolution range () | 501.40 (1.431.40) |
No. of unique reflections | 12169 (802) |
No. of observed reflections | 12169 |
Completeness (%) | 100 (100) |
Multiplicity | 23.8 (13.9) |
I/(I) | 18.5 |
R merge | 0.061 (0.371) |
Data-processing software | HKL-2000 |
Phasing method | Molecular replacement |
Starting model data set | PDB entry 2rh2 |
Solution software | REFMAC |