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. 2011 Oct 27;67(Pt 11):1440–1442. doi: 10.1107/S1744309111036694

Table 1. Data-collection statistics.

Values in parentheses are for the highest resolution shell.

Beamline BL17U1
Wavelength (Å) 0.9792
Crystal-to-detector distance (mm) 300
Oscillation range per frame (°) 1
Images taken 360
Resolution (Å) 50.0–2.7 (2.8–2.7)
Space group P3121
Mosaicity (°) 0.349
Unit-cell parameters (Å) a = b = 72.2, c = 260.4
No. of molecules per asymmetric unit 6
Matthews coefficient (Å3 Da−1) 2.48
Solvent content (%) 50.4
No. of observed reflections 482075
No. of unique reflections 41581
Completeness (%) 100.0 (100.0)
Multiplicity 11.6 (11.6)
Average I/σ(I) 29.3 (7.9)
Rmerge (%) 8.2 (32.6)

R merge = Inline graphic Inline graphic, where I i(hkl) is the intensity of observation i of reflection hkl.