Table 1. Data-collection statistics.
Beamline | BL17U1 |
Wavelength (Å) | 0.9792 |
Crystal-to-detector distance (mm) | 300 |
Oscillation range per frame (°) | 1 |
Images taken | 360 |
Resolution (Å) | 50.0–2.7 (2.8–2.7) |
Space group | P3121 |
Mosaicity (°) | 0.349 |
Unit-cell parameters (Å) | a = b = 72.2, c = 260.4 |
No. of molecules per asymmetric unit | 6 |
Matthews coefficient (Å3 Da−1) | 2.48 |
Solvent content (%) | 50.4 |
No. of observed reflections | 482075 |
No. of unique reflections | 41581 |
Completeness (%) | 100.0 (100.0) |
Multiplicity | 11.6 (11.6) |
Average I/σ(I) | 29.3 (7.9) |
Rmerge† (%) | 8.2 (32.6) |
R merge = , where I i(hkl) is the intensity of observation i of reflection hkl.