| Bruker Kappa APEXII CCD diffractometer | 2719 independent reflections |
| Radiation source: fine-focus sealed tube | 1972 reflections with I > 2σ(I) |
| graphite | Rint = 0.037 |
| φ and ω scans | θmax = 28.3°, θmin = 2.7° |
| Absorption correction: multi-scan (SADABS; Bruker, 2001) | h = −13→13 |
| Tmin = 0.492, Tmax = 0.771 | k = −12→7 |
| 12176 measured reflections | l = −14→14 |