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. 2011 Jul 23;67(Pt 8):o2078. doi: 10.1107/S1600536811027930
Refinement on F2 Primary atom site location: structure-invariant direct methods
Least-squares matrix: full Secondary atom site location: difference Fourier map
R[F2 > 2σ(F2)] = 0.032 Hydrogen site location: inferred from neighbouring sites
wR(F2) = 0.079 H atoms treated by a mixture of independent and constrained refinement
S = 1.01 w = 1/[σ2(Fo2) + (0.0403P)2 + 0.1092P] where P = (Fo2 + 2Fc2)/3
2719 reflections (Δ/σ)max = 0.001
152 parameters Δρmax = 0.40 e Å3
0 restraints Δρmin = −0.35 e Å3