| Rigaku Mercury diffractometer | 2601 reflections with F2 > 2σ(F2) |
| Detector resolution: 7.31 pixels mm-1 | Rint = 0.025 |
| ω scans | θmax = 27.5° |
| Absorption correction: multi-scan (REQAB; Jacobson, 1998) | h = −10→10 |
| Tmin = 0.942, Tmax = 0.950 | k = −13→13 |
| 7636 measured reflections | l = −7→10 |
| 2752 independent reflections |
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