Oxford Diffraction Xcalibur S diffractometer | 2888 independent reflections |
Radiation source: Enhance (Mo) X-ray Source | 2272 reflections with I > 2σ(I) |
graphite | Rint = 0.021 |
Detector resolution: 8.4353 pixels mm-1 | θmax = 25.0°, θmin = 3.3° |
ω scans | h = −5→5 |
Absorption correction: multi-scan (CrysAlis RED; Oxford Diffraction, 2009) | k = −14→14 |
Tmin = 0.877, Tmax = 1.000 | l = −16→9 |
10043 measured reflections |