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. 2011 Jul 30;67(Pt 8):o2209. doi: 10.1107/S1600536811029801
Bruker SMART CCD area-detector diffractometer 2983 independent reflections
Radiation source: fine-focus sealed tube 1404 reflections with I > 2σ(I)
graphite Rint = 0.070
φ and ω scans θmax = 27.2°, θmin = 1.4°
Absorption correction: numerical (SADABS; Bruker, 2003) h = −15→14
Tmin = 0.861, Tmax = 0.865 k = −4→4
11154 measured reflections l = −38→37