Bruker SMART CCD area-detector diffractometer | 2983 independent reflections |
Radiation source: fine-focus sealed tube | 1404 reflections with I > 2σ(I) |
graphite | Rint = 0.070 |
φ and ω scans | θmax = 27.2°, θmin = 1.4° |
Absorption correction: numerical (SADABS; Bruker, 2003) | h = −15→14 |
Tmin = 0.861, Tmax = 0.865 | k = −4→4 |
11154 measured reflections | l = −38→37 |