TABLE 3.
Observed masses (m/z) and structural breakdown of peaks from electrospray ionization mass spectrometry of TFA-digested TvLG and TFA-digested and reduced TvLG
m/z | TFA-digested TvLG |
m/z | TFA-digested and reduced TvLG |
||||||
---|---|---|---|---|---|---|---|---|---|
Xylose | Rhamnose | Galactose | GlcNAc | Xylose | Rhamnose | Galactose | GlcNAc | ||
488 | 0 | 1 | 0 | 1 | 450 | 1 | 0 | 1 | 0 |
518 | 0 | 0 | 1 | 1 | 464 | 0 | 1 | 1 | 0 |
662 | 0 | 2 | 0 | 1 | 535 | 0 | 0 | 1 | 1 |
692 | 0 | 1 | 1 | 1 | 709 | 0 | 1 | 1 | 1 |
722 | 0 | 0 | 2 | 1 | 739 | 0 | 0 | 2 | 1 |
763 | 0 | 0 | 1 | 2 | 780 | 0 | 0 | 1 | 2 |
822 | 1 | 2 | 0 | 1 | 855 | 2 | 0 | 1 | 1 |
836 | 0 | 3 | 0 | 1 | 869 | 1 | 1 | 1 | 1 |
852 | 1 | 1 | 1 | 1 | 913 | 0 | 1 | 2 | 1 |
866 | 0 | 2 | 1 | 1 | 940 | 1 | 0 | 1 | 2 |
896 | 0 | 0 | 3 | 1 | 954 | 0 | 1 | 1 | 2 |
937 | 0 | 1 | 1 | 2 | 984 | 0 | 0 | 2 | 2 |
967 | 0 | 0 | 2 | 2 | 1114 | 1 | 1 | 1 | 2 |
996 | 1 | 3 | 0 | 1 | 1144 | 1 | 0 | 2 | 2 |
1010 | 0 | 4 | 0 | 1 | 1158 | 0 | 1 | 2 | 2 |
1040 | 0 | 3 | 1 | 1 | 1188 | 0 | 0 | 3 | 2 |
1170 | 1 | 4 | 0 | 1 | 1229 | 0 | 0 | 2 | 3 |
1184 | 0 | 5 | 0 | 1 | 1433 | 0 | 0 | 3 | 3 |
1214 | 0 | 4 | 1 | 1 | 1607 | 0 | 1 | 3 | 3 |
1255 | 0 | 4 | 0 | 2 | 1637 | 0 | 0 | 4 | 3 |
1301 | 1 | 1 | 2 | 2 | |||||
1344 | 1 | 5 | 0 | 1 | |||||
1358 | 0 | 6 | 0 | 1 | |||||
1416 | 0 | 0 | 3 | 3 | |||||
1429 | 0 | 5 | 0 | 2 |