Table 1. Crystal Data, Data Collection, and Refinement Statistics.
space group | orthorhombic P212121 |
cell parameters (Å) | a = 25.64, b = 40.31, c = 65.93 |
temperature of data collection (° C) | –170 |
wavelength (Å) | 0.9785 |
max resolution (Å) | 1.1 |
unique reflections | 27920 |
completeness all/1.14–1.10 Å (%) | 97.8/95.8 |
redundancy all/1.14–1.1 Å | 10.6/6.9 |
I/σ (I) all/1.14–1.1 Å | 61.26/4.8 |
Rmerge all/1.14–1.10 Å | 0.048/0.394 |
Rwork | 0.161 |
Rfree | 0.195 |
number of DNA atoms | 486 |
number of water molecules | 133 |
number of ions | 1 Mg2+ |
4 Na+ | |
rms distances (Å) | 0.024 |
rms angles (°) | 1.95 |