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. Author manuscript; available in PMC: 2012 Aug 31.
Published in final edited form as: J Am Chem Soc. 2011 Aug 9;133(34):13718–13730. doi: 10.1021/ja205568r

Figure 2.

Figure 2

Steady-state FTIR spectra (bottom) of saturated Re′-OEt in acetonitrile recorded during bulk reduction using an OTTLE cell. Arrows indicate spectral changes that occur upon reduction. The difference in absorbance between the fully reduced species and the initial species is also shown (top).