Table 1. Experimental conditions and data-collection statistics.
Values in parentheses are for the highest resolution shell.
| Wavelength (Å) | 1.29 |
| Temperature (K) | 100 |
| Space group | C2 |
| Unit-cell parameters (Å, °) | a = 121.61, b = 95.00, c = 72.10, α = γ = 90, β = 114.19 |
| Resolution limits (Å) | 20–2.8 (2.95–2.80) |
| Total reflections | 72099 (10599) |
| Unique reflections | 18458 (2681) |
| Completeness (%) | 99.7 (100) |
| Rmerge† (%) | 14.3 (52.9) |
| Mean I/σ(I) | 7.7 (2.6) |
| Multiplicity | 3.9 (4.0) |
| Wilson B factor (Å2) | 47.8 |
| VM (Å3 Da−1) | 2.81 |
| Z | 4 |
| Solvent content (%) | 56 |
†
R
merge = 
× 100%, where Ii(hkl) is the measured intensity and 〈I(hkl)〉 is the average intensity over symmetry-equivalent reflections.