Table 1. Data-collection statistics.
Values in parentheses are for the last shell.
| Beamline | Spring-8 BL26B1 |
| Wavelength (Å) | 1.0 |
| Resolution range (Å) | 50.0–3.0 (3.05–3.00) |
| Space group | P41 |
| Unit-cell parameters (Å) | a = b = 82.2, c = 233.2 |
| Total No. of reflections | 1169323 |
| No. of unique reflections | 30477 |
| Completeness (%) | 98.2 (95.9) |
| Molecules per asymmetric unit | 4 |
| Solvent content (%) | 43.5 |
| Average I/σ(I) | 10.6 (2.4) |
| Rmerge† (%) | 11.5 (38.2) |
| Rp.i.m.‡ (%) | 9.5 (35.5) |
| Multiplicity | 4.2 (3.1) |
R
merge =
.
R
p.i.m. =
, where Ii(hkl) is the intensity of reflection hkl,
is the sum over all reflections,
is the sum over i measurements of reflection hkl and 〈I(hkl)〉 is the weighted average intensity of all observations i of reflection hkl.