TABLE 1.
Data collection and refinement statistics for structure determination of the UreF-UreH complex
Values in parentheses correspond to the highest resolution shell.
| Protein Data Bank code | 3SF5 |
| Space group | P212121 |
| Unit cell parameters | 70.6 Å, 70.7 Å, 205.5 Å |
| Wavelength | 1.54187 Å |
| Resolution | 50.0 to 2.50 Å (2.65 to 2.50 Å) |
| No. of unique reflections | 36,388 (5529) |
| Redundancy | 7.9 (7.3) |
| Completeness | 99.1% (95.0%) |
| Mosaicity | 0.25° |
| Average I/σ | 23.02 (7.30) |
| Rmerge | 0.057 (0.179) |
| Rwork | 0.173 (0.206) |
| Rfree | 0.217 (0.292) |
| Average B-factor | 31.8 Å2 |
| Root mean square bond lengths | 0.003 Å2 |
| Root mean square angles | 0.692° |
| Ramachandran analysis | Preferred 97.3%; allowed 99.8% |
| Diffraction precision index | 0.2558 Å |