Table 2.
Cycle Time [s] | ||
---|---|---|
12 | 21 | |
2tg [s] a | 9 | 18 |
2tre-eq [s] b | 3 | 3 |
2L [cm] c | 3.3 | 3.3 |
2F [mL/min] d | 3.0 | 3.0 |
Vloop [μL] e | 20 | 34 |
2φi f | 0 | 0 |
2φf g | 1.0 | 1.0 |
2nc, measured h | 24 | 32 |
Column is 3.3 cm long by 2.1 mm i.d. packed with ZirChrom-CARB 3 μm particles. Temperature is 110 °C.
Gradient time;
Re-equilibration time;
Column length;
Flow rate;
Sample loop volume;
Initial eluent strength;
Final eluent strength;
Second dimension peak capacity calculated by eq. (8) using measured average peak width.