| Bruker APEXII CCD diffractometer | 9327 independent reflections |
| Radiation source: sealed tube | 6401 reflections with I > 2σ(I) |
| graphite | Rint = 0.098 |
| Detector resolution: 512 pixels mm-1 | θmax = 28°, θmin = 2.0° |
| φ and ω scans | h = −10→6 |
| Absorption correction: multi-scan (SADABS; Bruker, 2004) | k = −15→16 |
| Tmin = 0.887, Tmax = 0.937 | l = −27→27 |
| 26016 measured reflections |